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The Theory. Supercritical Fluid Extraction (SFE) is the process of separating one component (the extractant) from another (the matrix) using supercritical fluids as the extracting solvent. Extraction is usually from a solid matrix, but can also be from liquids. SFE can be used as a sample preparation step for analytical purposes, or on a larger scale to either strip unwanted material from a product (e.g. decaffeination) or collect a desired product (e.g. essential oils). Carbon dioxide (CO2) is the most used supercritical fluid, sometimes modified by co-solvents such as ethanol or methanol. Extraction conditions for supercritical CO2 are above the critical temperature of 31°C and critical pressure of 74 Bar. Addition of modifiers may slightly alter this. The discussion below will mainly refer to extraction with CO2, except where specified. Chemtron and Supercritical Extraction. It is great pleasure introduce ourselves as Single Source for Design, Supply, and Installation & Commissioning of Super Critical Extraction plants based on Co2 Gas of various sizes like 0.5 liter capacity. We are work in this technology for the past 5 years. It started for academic intrest and now we have designed and supplied 10 ltr pilot plant to customers. Chemtron Science Lab Pvt Ltd is ISO 9001 certified and has a existence of 17 years as on 2009 in the business of gases. Services provide by Chemtron in contract research. We also offer a variety of service for supercritical extraction including extraction of material on job basis. We also undertake research samples of commercial scale production, and develop optimum condition for extraction and commercial scale planning and project report for finance option from commercial banks. Please contact us and give a detailed description of your needs.. We can provide complete solution for extraction by Supercritical Co2 method that includes:
The Extraction Process The residue consists of all other substances that are present in the feed the oil soluble substances are a range of chemicals with different molecular weights. They exhibit a solubility pattern inversely proportional to their molecular weights at any given temperature and pressure. The presence of different organic substituted groups also affects the solubility. Lower molecular weight components are extracted faster and have higher solubility in CO2, while higher molecular weight components have a lower solubility and consequently lower extraction rates. Once the extract is obtained, it is clarified, and water is separated out and the material is filled in containers. This extract is called the total extract. Supercritical fractionation Sometimes there is a need to separate the low boiling essential oils or other active ingredients from the high boiling components of the combined total extract. This can be done using our liquid supercritical fractionation column. This is a continuous operation w.r.t. both the extract and CO2. The bottom end of the fractionator is a mixture of un-extracted material. The top section carries the extracted low boiling components along with CO2.
Lab Scale
10 L Pilot plant
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